Selective pressurized liquid extraction of polychlorinated biphenyls in sediment.
A selective pressurized liquid extraction procedure (SPLE) was developed for a fast determination of polychlorinated biphenyls in sediment. The final method was performed at 100 degrees C with heptane/dichloromethane (90:10, v/v) as extraction solvent for 2 x 5 min. Sulfuric acid impregnated silica was placed downstream of the sample in the extraction cell to remove interfering components. This si